简介：PolycrystallinesamplesofLa12x(Sr12yAgy)xMnO3(y=0.0,0.2,0.4,0.6,1.0)werepreparedbythesolid-statereactionmethod.ThetemperaturestabilityofmagnetoresistanceandmagnetoresistanceenhancementinLa1-x(Sr1-yAgy)xMnO3systemwithbothunivalentandbivalentelementsdopedatAsiteandwithunchangedvalueofMn3+/Mn4+ratiowereexploredthroughthemeasurementsofX-raydiffractionpatterns,magnetiza-tion-temperature(M-T)curves,resistivity-temperature(q-T)curvesandmagnetoresistance-temperature(MR-T)curves.Theresultsareasfollows:therearetwopeaksintheq-TcurvesofthesampleswithAgdoping,oneiscausedbyresistancechangeduringtheparamagnetism-ferromagnetismtransition,andtheotherisfromboundary-dependentscatteringofconductionelectronsontheboundariesofgrains.ThepeakvalueofMRincreaseswithincreasingAgdopingcontent,anditincreasesfrom8.2%fory=0.2to29.6%fory=1.0underthemagneticfieldofB=0.8T;MRremainsaconstantof12%inthetemperaturerangeof218-168Kforthesamplewithy=1.0,andthetemperaturestabilityofMRisinfavorofthepracticalapplicationofMR.

简介：ThestructureandelectrochemicalpropertiesofanewlowcobalthydrogenstorageelectrodealloysLa1-xLixNi3.2Co0.3Al0.3(0≤x≤0.2)wereinvestigatedwithadifferentadditionsofLiinreplacementofLa.WiththeincreaseofLicontentsthemaximumdischargecapacityincreasesfrom240mAh·g-1(x=0)to328.4mAh·g-1(x=0.1)andthecyclestabilityisimprovedcorrespondingly.ThecapacitydecaycanremaiN28.6%(x=0.2)after230charge/dischargecycles.Thehighratedischarge(HRD)abilityofthealloys(x≤0.1)isimprovedandthebestHRDis34.1%(x=0.1)underthedischargecurrentdensity1200mA·g-1.ItisfoundthatthepreparedalloysarebasicallycomposedofLaNi5asmatrixphaseandLaNi3assecondphase(x≤0.1).ButtheabundanceofLaNi3phasedramaticallydecreaseswithincreasingx.Whenx=0.2,anewphaseAl(NiCo)3isformed.

简介：本文讨论了叶蜡石密封边的结构的变化。

简介：BasedontheMiedemamodelandExtendedMiedematheory,theformationenergiesofdifferentsolutecomponentsinEr-XbinarysystemandAl-Er-Xternarysystemswerecalculated.TheresultsshowthatthevariationoferbiumcontenthaslittleinfluenceonthechancerateoftheformationAl-ErcompoundintheAl-Mg-Mn-Zr-Ersystem.ThecalculatedformationenergiesintheEr-XbinarysystemandAl-Er-XternarysystemsindicatethatAl3Erphasecantakepriorityofdepositing,Al-Er-Zrternarycompoundsmayalsofoundwhichagreeswiththeexperimentalresultsinreferences.TheconsistencyofcalculationandexperimentprovesthattheintermetalliccompoundsintheAl-Mg-Mn-Zr-ErsystemcanbepredicteddirectlybycalculatingtheformationenergiesofthereactionsinEr-XbinarysystemandAl-Er-XternarysystemswiththeMiedemamodelandExtendedMiedematheory.

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简介：日前，山东黄金集团所属焦家金矿“矿山出矿用折叠漏斗”实用新型专利技术获得国家知识产权局颁发的《发明专利证书》。这是该矿继今年6月份获得“井下充填专用胶结材料的制备方法”《发明专利证书》后的又一项实用新型专利。该专利主要技术思路是提供一种矿山井下出矿实用漏斗，通过结构改进把外侧漏斗变成可折叠的活式漏斗，从而使内侧漏斗的矿料可以通过电机车搬运，

简介：用XPS技术和X射线衍射方法检测了复合片中各个元素的结合能与晶体结构的变化，讨论了复合片与质量有关的问题。

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简介：用X衍射实验测量了灰色叶蜡石、灰白色叶蜡石、黄色叶蜡石、深红色叶蜡石的结构和杂质。

简介：GaxIn1-xAs1-ySbyalloyshavebeengrownbyatmosphericpressureMOCVDonn-GaSb（Te-doped）substrate.Thesohdcompositionwasdeterminedbyusingelectronmicroprobe.ThealloysofGalnAsSbwithcompositioninmiscibilitygapweresuccessfullygrown.TheopticalpropertiesofGaxIn1-xAs1-ySbylaverswerecharacterizedbythephotoluminescenceandtheinfraredabsorption.Thespectralresponsesofp+-GaInAsSb/p-GaxIn1-xAs1-ySby/n-GaSbdetectorsshowedwavelengthcutoffat2.4μmanddetectivity-D*=5×108cmHz1/2/Watroomtemperature.

简介：Inthisinvestigation,themechanicalpropertiesandlow-temperaturefracturetoughnessofAPI5LX65offshorepipelineweldedjointswerestudied.StructureIntegrityAssessmentProcedure(SINTAP)-FailureAssessmentDiagram(FAD)methodwasappliedtothepipestructurewithsurfaceflawattheweldtoe.AccordingtotheISOstandardBS7448,theCTODfracturetoughnessoftheweldedjointswasdeterminedatthetemperatureof0℃.Fortheheat-affectedzone(HAZ)specimens,post-testmetallographicanalysiswasperformedtoverifythatthetipofthecrackwaslocatedinthecoarsecrystalzoneinordertoconfirmthevalidityoftheaboveresults.Thefailurelinesofanalysislevel1and3ofweldmetalwerederivedfromtheresultsofthemechanicalpropertytest.Theassessmentwasperformed,consideringthemaximumlaystress,residualstressconservativelyassumedtobeuniformtensilestress,andminimumCTODvalue.Theresultsoftheassessmentshowedthatpipelinestructurewithasurfaceflaw(theheightandlengtharerespectively2.2mmand5mm)attheweldtoeissafe.ThisstudylaysthefoundationofapplicationofSINTAPtopipelinestructureassessment.

简介：Ｘ－ｒａｙＤｏｕｂｌｅ－ｃｒｙｓｔａｌＤｉｆｆｒａｃｔｏｍｅｔｅｒｗｉｔｈＨｏｒｉｚｏｎｔａｌＳｌｉｔｓａｎｄＩｔｓＡｐｐｌｉｃａｔｉｏｎｓＸｕＪｉｎｇｙａｎｇａｎｄＺｈｕＮａｎｃｈａｎｇ徐景阳，朱南昌（ＳｈａｎｇｈａｉＩｎｓｔｉｔｕｌｅｏｆＭｅｔａ...

简介：涡轮叶片在X射线无损检测时，X射线底片上存在黑白线显示。运用视频显微镜、光学显微镜对叶片黑白线显示部位的表面形貌和显微组织进行了观察分析。结果表明，黑白线显示是由于陶瓷型芯表面错位或微裂纹，使得叶片内腔表面存在具有一定高差的台阶。而陶瓷型芯表面形成错位或微裂纹主要与型芯表面质量和材料高温强度有关。通过控制陶瓷型芯材料纯度和粒度，选择合适的工业氧化铝填料以及加强压芯工艺参数和修芯工艺过程控制，提高型芯表面质量和高温强度，可明显减少甚至消除X射线黑白线显示。

简介：LayeredcathodematerialLiCo1/3Ni1/3Mn1/3O2wassynthesizedbyPechiniprocess,andinvestigatedusingX-raydiffraction(XRD),scanningelectronmicroscopy(SEM)andgalvanostaticcharge/dischargecycling.Thesampleiswell-crystallizedandhasaphase-purea-NaFeO2structure.Theparticlesizesareuniform,anddistributedintherangeof20-200nm.TheinitialdischargecapacityoftheLi/LiCo1/3Ni1/3Mn1/3O2cellwasabout149mAh·g-1whenitwascycledatavoltagerangeof4.5-2.3Vwithaspecificcurrentof0.25mA.Theresultisbetterincomparisonwithsolid-statesolutionmethod.Thesyntheticprocedurewasdiscussed.Threemajorreactions:chelation,esterification,andpolymerizationsuccessivelyoccurred.

简介：MgTixNi(x=0,0.1,and0.2)alloysweresuccessfullypreparedbymechanicalalloying(MA),andtheinfluenceofmillingtimeontheelectrochemicalcharacteristicsoftheelectrodeswasdiscussed.MgTixNialloysafter90hmillingdisplayedthebestelectrochemicalperformance.TheX-raydiffractionpatternsshowedthatthealloyball-milledfor90hwasamorphouswithawideneddiffractionpeak.Thecharge-dischargetestsindicatedthatthesealloyshadgoodelectrochemicalactivationproperties,andtheMgTi0.2Nialloyelectrodeexhibitedthebestcycleperformance.TheinitialdischargecapacityoftheMgTi0.2Nialloyreachedupto401.1mAh·g-1,andtheretentionrateofcapacitywas31.0%after30cycles,muchhigherthanthatofMgNi(17.3%).TheTafelpolarizationcurvesrevealedthatTiadditioncouldenhancetheanticorrosionperformanceofthesealloysinalkalisolution,whichwasresponsiblefortheamelioratedcyclicstabilityofthesealloyelectrodes.

简介：X-raydiffraction(XRD)anddifferentialscanningcalorimetry(DSC)wereusedtoinvestigatethecrystallizationprocessofamorphousAl90TMxCe10-x(atomfractionin%;TM=FeorNi;x=3,5)alloys.AgingeffectswereexaminedbyX-raydiffraction.ThestructurecorrespondingtotheprepeakfortheamorphousAl90Fe5Ce5alloyismorestablethantheamorphousmatrix,butitisnotstableforamorphousAl90Ni5Ce5alloyduringthefirstcrystallizationstageandevendecomposesatroomtemperature.AlthoughbothAl-NiandAl-Fehavestrongchemicalbonding,thecrystallizationonsettemperatureofamorphousAl-Fe-CealloysismuchhigherthanthatofamorphousAl-Ni-Cealloys,whichislikelycausedbythedifferentstabilityofthestructurecorrespondingtotheprepeak.ThecrystallizationonsettemperatureincreasesasCe/NiratioincreasesinamorphousAl90NixCe10-xalloys,whereasitdecreasesasCe/FeratioincreasesinamorphousAl90FexCe10-xalloys.AbetteratomicpackingproducesasCecontentincreasesbecauseofthesizemismatchinAlNi-CesystemsandasFecontentincreasesbecauseoftheincreasingFecentralstructuralunits.

简介：本文将介绍新研制的一种用于人造金刚石合成的触媒合金JX－1，其合成效果明显优于Ni70Mn25Co5，且金刚石的颜色呈金黄色，金刚石的TI、TTI值较高，磁化率较低。

简介：转子工作时不仅需要承受高速旋转（3000r／min）所产生的巨大离心力，同时还承受扭转和弯曲的应力．是汽轮机上重要的安全部件。因此，要求其强度高、韧性好、组织性能均匀、残余应力小等，探伤执行标准为JB／T1265-2002。转子的锻造难度大干一般轴类锻件．因此必须要有可靠的工艺、先进的设备和熟练的操作工人才能保证锻出优质的转子。

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