Trivalentdysprosium(Dy3+)activatednanocrystallineyttriumvanadate(YVO4)phosphorwassynthesizedviaco-precipitationmethod.ThepreparedsampleswerecharacterizedbyX-raydiffraction(XRD),Fouriertransforminfraredspectroscopy(FTIR),scanningelectronmicroscopy(SEM),opticalabsorptionandphotoluminescence(PL)techniques.TheXRDpatternsrevealthetetragonalcrystallinephase.SEMimagesrevealthatDydopedYVO4nanocrystalsareagglomerated.EDAXconfirmstheformationofYVO4:Dy.FTIRspectrumshowstwostrongabsorptionbandsat459and761cm-1.Opticalabsorptionspectrumshowedthesurfacedefectsintheas-preparedsamples.ThePLemissionspectrumshowstwocharacteristicemissionbandsat485and575nm.Thestrongyellowemissionpeakat575nmisassignedto4F9/2→6H13/2hypersensitivetransitionofDy3+ions,StudyofCIEchromaticitydiagramindicatesthesuitabilityofthephosphorforthedevelopmentofyellow-greenLEDs.