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170 个结果
  • 简介:本文用循环伏安测温(CVT)热电化学外推方法首次研究了CuS阳极过程动力学性质。实验的塔费尔斜率b值与按迟缓放电机理所导出的Tafel斜率b的理论计算值相符。

  • 标签: CVT Cu_2S Tafel 斜率b
  • 简介:通过对氯化钻溶液生产实践的论证,本文对生产氯化钴溶液萃取过程中影响其品质因素进行了分析和总结,提出了在现有工艺和技术条件下,生产氯化钻溶液在萃取过程中的最佳温度、pH值、皂化率及流比。

  • 标签: 萃取 温度 PH值 皂化率 流比
  • 简介:Glasseswiththecompositionof65GeO212Ga2O3-10BaO-8Li2O-5La2O3(molarratio)dopedwith1.526wt.%,3.006wt.%,5.836wt.%,11.028wt.%,and15.678wt.%Tm2O3,respectively,werefabricatedbyconventionalmeltingmethod.AccordingtotheabsorptionspectraandtheJudd-Ofelttheory,theJ-Ostrengthparameters(Ω2,Ω4,Ω6)werecalculated,withwhichtheradiativetransitionprobabilities,branchingratiosandradiativelifetimeswereobtained.Theinfraredemissionspectra(with808nmLDexcitation)at~1.47and~1.8μmofvariousconcentrationsofTm3+-dopedglasseswerestudied.Theemissionintensityat~1.8μmreachedtothemaximumwhentheTm2O3-dopingconcentrationwasneartobe~3.006wt.%(1.0mol.%),andthendecreasedasdopingconcentrationincreasedfurther.Themechanismofthefluorescenceintensitychangewasexplainedwiththecross-relaxationeffectandtheconcentrationquenchingeffectofTm3+.Meanwhile,accordingtoMcCumbertheory,theabsorptionandemissioncross-sectionscorrespondingtothe3F4→3H6transitionsofTm3+at1.8μmwasobtained.ForTm3+-dopedgermanateglasses,themaximumemissioncross-sectionreachedavaluehigherthanthatre-portedforfluorozircoaluminateglasses.Itisexpectedtobeafavorablecandidatehostfor~2.0μmmid-inflatedlaserbecausetheglassshowsfavorableopticalspectra.

  • 标签: Tm3+-doped germanium-gallate GLASSES spectral properties cross
  • 简介:Theaimofthisresearchistopulseco-depositnano-CeO2particlesintoNi-W-Balloycoatingsinordertoimprovethesurfaceproperties.Theinfluenceofpulsefrequencyanddutycircleondepositionrate,microhardnessandmicrostructures,andtheinfluenceofheattreatmenttemperatureonphasestructures,microhardnessandabrasivityofNi-W-B-CeO2compositecoatingswereinvestigated.Theresultsindicatedthatthepulseco-depositionofnickel,tungsten,boronandnano-CeO2particlefromthebathwhichnano-CeO2particlewassuspendedbyhighspeedmechanicalstirringledtotheNi-W-B-CeO2compositecoatings,possessingbettermicrohardnessandabrasionresistancewhenheat-treatedat400℃for1h.Themicrohardnessas-depositedwith636Hzandthedepositionratewith0.0281mm·h-1wasthehighestatpulsefrequencywith1000Hzandpulsedutycirclewith10%.Microstructuresanalysisdisplaysthatdecreasingpulsedutycycleleadstorefinementingrainstructuresandtheimprovementofmicrostructures.X-raydiffractionshowsthatthecompositecoatingas-depositedwasmainlyintheamorphousstateandpartiallycrystallized,butwhenheattreatedat400℃,thecrystallizationtrendwasstrengthenedfurther.

  • 标签: pulse ELECTRODEPOSITION composite coatings deposition rate
  • 简介:通过运用工艺流程参数梳理,分析影响余热发电的制约原因,找出关键影响因素,并提出必要可行的措施,包括优化原料结构、强化烧结生产操作、完善现有工艺条件以及加强设备管理等.经过一系列有效措施的制定并实施后,余热发电量明显提升,在降低工序能耗的同时实现了稳定高效生产.

  • 标签: 余热发电 厚料层 优化工艺 密封改造
  • 简介:ElectronMicroscopicIn-situObservationforPreparationofUltrafineLaO3NanophasePowderGaoYuzun(高愈尊),LiYonghong(李永洪),ZhangTaisong...

  • 标签: La2O3 NANOPHASE Insitu OBSERVATION High voltage
  • 简介:OpticalabsorptionandemissionintensitiesofNd3+ioninKLu(WO4)2crystalwereinvestigated.BasedontheJudd-Offelttheory,wecalculatedthefollowingspectralparameters:phenomenologicalintensityparametersΩ2=5.567×10–20,Ω4=3.597×10–20,andΩ6=3.800×10–20cm2.Theradiativelifetimeoflevels4F3/2was182.58μs.Thefluorescencebranchingratioforthetransition4F3/2→4I11/2was46.98%.Inaddition,theradiativetransitionprobabilitiesAJ,J’,oscillatorstrengthsPJ,J’andthevaluesofinte...

  • 标签:
  • 简介:StudyonMorphologyofSurfaceofLargeAreaYBCOThinFilmsonZr(Y)OSubstrateWangRuikun(王瑞坤),SunLihong(孙丽虹),LiuHongfei(刘鸿飞)WangXiaopi?..

  • 标签: Yba2Cu3Oy THIN film SURFACE MORPHOLOGY
  • 简介:通过对2号常化酸洗线活套支撑小车弹簧式力矩卷筒进行了改进,提高了弹簧式力矩卷筒本体的强度及钢丝绳的破断拉力强度,延长了弹簧式力矩卷筒的使用寿命,降低了力矩卷筒失效频率,提高了设备的有效开动率,为设备点检和维护创造了良好的条件,满足了正常生产的管理要求,确保了生产的正常运行。

  • 标签: 力矩卷筒 拉力 破断拉力
  • 简介:采用高温固相法合成尖晶石LiMn2O4,并以化学沉积方式对其进行包覆氧化钴的表面处理。通过X射线衍射(XRD)、扫描电镜(SEM)等技术对表面处理前后的LiMn2O4进行表征,分析了表面处理后LiMn2O4物理特性的变化,并结合电化学性能测试,研究了表面处理及其工艺和条件对LiMn2O4电化学容量与循环性能的影响。结果表明,表面处理后LiMn2O4循环性能显著提高。随氧化物含量的增加,循环性能提高,容量降低。未经表面包覆的LiMn2O4首次充放电容量为108.13mAh/g,50次循环充放电后容量衰减26.3%。500℃加热处理的表面包覆0.5%、2%氧化钴的LiMn2O4首次循环放电容量各为118.38mAh/g、115mAh/g,经过50次充放电循环后,容量分别降低8%、7%。

  • 标签: LIMN2O4 蓄电池 氧化钴 表面处理 电化学性能
  • 简介:高度有效的Tb3+激活SrAl2O4黄磷被一个联合combustionsolid状态反应方法综合。SrAl2O4的先锋:Tb3+黄磷经由一个燃烧过程被准备,然后同样准备的粉末被加热在一减少在1250点的激活的碳周围??慥獲?

  • 标签: 燃烧分析 SrAl2O4: TB^3+ 结晶度 稀土
  • 简介:DyPt2filmswerepreparedbyalternatedepositionthinDyandPtlayersonglasssubstratesbyDCmagnetocontrolledsputteringmethod.TheXRDdataindicatedthatforas-depositedDy/Ptfilms,andtheperiodiclayeredstructuresalongthicknessdirectionwereevidencedwithlowangleX-rayscattering.Withincreasingannealingtemperature,thecompoundsofDyPt,DyPt2andDyPt3wereformedsuccessivelyattemperaturerangingfrom300to400℃.ItwasfoundthatthecompositionreactionDyPt+DyPt3→2DyPt2tookplaceat500℃.Afterannealingat500℃for1h,thecompoundsDyPtandDyPt3transformedcompletelyintotheDyPt2compound.

  • 标签: Dy/Pt thin film microstructure heat treatment
  • 简介:主要介绍了265m2烧结机自动化控制系统的结构及其主要控制功能,分析了故障诊断与报警、联锁的设计特点.该系统投运两年多来,运行平稳、质量可靠,取得了较好的成效.

  • 标签: 烧结机 自动化 PLC控制系统 设计
  • 简介:Forthegoalofsulfurrecovery,mostmethodsareaimedatthetailgaswithhigh-concentrationH2S,butfeweffectivemethodsareusedforlow-concentrationH2S.Inthiswork,Low-concentrationH2Scouldbepurifiedwellbyliquidphasecatalyticoxidation(LCO),andthesulfurresourcecouldalsoberecovered.TheabsorptionsolutionwaspreparedbyFeCl3andsulfosalicylicacid.Undertheexperimentalconditions,theconversionofH2StoScouldbemaintainedabove94%at60℃.InordertoenhancetheeconomicalefficiencyofLCOmethod,theabsorptionsolutionwasmodifiedbydopingCe,andaseriesofexperimentsweredesignedtoinvestigateitsperformance.TheresultsshowedthattheconversionofH2Shadnoobviousimprovement,butabove98%conversioncouldbegainedat60℃,andtheH2Sconversionratewasenhanced.TheoptimumadditionqualityofCe(NO3)3was0.08gto50mlFe3+solution.

  • 标签: HYDROGEN SULFIDE liquid phase CATALYTIC OXIDATION
  • 简介:据行业网站报道,台湾烨联百分百转投资子公司“福建联德企业”的4条矿热炉(RKEF)镍铁生产线陆续运转,可于2月份全部投产,未来全产能可达到20万吨,可提供不锈钢厂炼钢使用。

  • 标签: 生产线 投产 镍铁 福建 预计 行业网站
  • 简介:印尼国有镍金生产商PTAnekaTambang(Antam)的高级官员周二表示,公司计划建一年产能为2—2.7万吨镍的镍铁冶炼厂。

  • 标签: 冶炼厂 镍铁 印尼 生产商
  • 简介:TheeffectsofUVAphotoirradiatedCe(Ⅳ)dopedTiO2nanoparticle(CDTP)onratcoloncarcinomacellline(C26)growth,cellcycledistribution,andmorphologywerestudiedbyMTTassay,FlowCytometry,andfluorescentstaining.Theresultsindicatethatabout64.6%cellsarekilledafter24hby180μg·ml-1CDTPwhen8minexposedtoUVA,over90%deadfor30mingroup,relativeto18.7%,41.5%ofTiO2atthesameconditionrespectively.Hoe33258stainingofthefixedcellsrevealstypicalapoptoticstructures(apoptoticbodies),andcellsarearrestedinG0/G1phase.

  • 标签: CERIUM DOPING TiO2 NANOPARTICLE TUMOR cell
  • 简介:ThemorphologyandcorrosionbehaviorofNi/Al2O3compositecoatingspreparedusingdouble-pulsedelectrodepositingtechniqueafteroxidizedunder800℃NaCldepositinairenvironmentwereanalyzedbyscanningelectricalmicroscope(SEM),X-raydiffraction(XRD)andenergydispersivespectrum(EDS).TheresultsshowedthatthecorrosionofallcompositecoatingswasacceleratedunderNaCldeposits,andthecorrosionproductswereratherporouswithpooradherencetothematrix.Al2O3particlesinthecoatingscanrefinethegrainsizeandimprovethehightemperaturecorrosionresistanceofthecoatings.Withinthetestscope,themoreAl2O3particlesinthecoatings,thelowercorrosionratescouldbeobtained,andthecorrosionmechanismwasalsodiscussed.

  • 标签: NI/AL2O3 composite coatings ELECTRODEPOSITION NACL corrosion
  • 简介:确定了合金成分,制定了中频感应熔炼工艺,开发了保证合金性能和质量的熔炼成分、成分均匀性以及杂质元素(O、N、H)精确控制技术;确定了MBA-2合金的铸造工艺、挤压工艺,最终产品各项性能指标均满足国标要求,形成了从合金熔炼、铸造、挤压及性能测试等关键工艺及技术。

  • 标签: MBA-2 同步器齿环管材 熔铸 挤压 检测