简介:TheeffectoftitaniumadditiononthemicrostructureandmechanicalpropertiesofbrassCu40Znhasbeenstudiedviathepowdermetallurgy(P/M)route.Thewater-atomizedCu40Zn—1.0wt%Tialloypowderwasconsolidatedatdifferenttemperaturesintherangeof400—600℃usingsparkplasmasintering(SPS)andhotextrusionsubsequently.Resultsshowthatthesuper-saturatedsolidsolutiontitaniumelementinrapidlycooledbrassCu40Znpowdercreatedhighchemicalpotentialforaprecipitatereaction,showingsignificantgrainrefinementeffectsontheconsolidatedCu40Znmatrix.Consequently,excellentmechanicalpropertieswereobtainedbyprecipitationhardeningandworkhardeningaftersinteringandextrusion,withyieldstrengthof390MPa,ultimatetensilestrengthof617MPa,andVickersmicro-hardnessof192HV,whichare28.7%,23.4%,and23.9%highervaluesthanthoseofextrudedCu40Znbrass,respectively.
简介:以硝酸铁为原料,三乙二醇(TEG)为溶剂,采用热分解法制备了γ-Fe2O3纳米粒子,通过X射线衍射fXRD)、差热-热重分析、N2吸附-脱附(BET)和磁性分析(VSM)等测试手段对制备的样品进行表征,并考察了硝酸铁浓度和反应时间对γ-Fe2O3晶粒尺寸及性能的影响,结果表明,硝酸铁在TEG中高温热分解后能够产生γ-Fe2O3纳米粒子,并且随着硝酸铁浓度和反应时间的增加,γ-Fe2O3纳米粒子的晶粒尺寸和饱和磁化强度都有增大的趋势。