简介:Microstructuresandmechanicalpropertiesoftransientliquidphase(TLP)bondedmagnesiummetalmatrixcomposite(MMC)jointsusingcopperinterlayerhavebeeninvestigated.Withanincreaseofbondingtimesfrom5minto50minatbondingtemperatureof510℃,theaverageconcentrationofcopperinthebondedzonedecreased,themicrostructureinthezonechangedfromCu,α-MgandCuMg2toα-Mg,CuMg2andTiC,andmechanicalpropertiesofthejointincreased.Theshearstrengthofthejointbondedat510℃for50minreached64MPaduetothemetallurgicalbondingofthejointandimprovingitshomogeneityofcompositionandmicrostructure.ItisfavorabletoincreasethebondingtimeforimprovingmechanicalpropertiesofTLPbondedmagnesiumMMCjoint.
简介:用等离子电解氧化(PEO)法在AZ91和AZ80镁合金表面制备涂层,研究在电解液中添加石墨纳米颗粒对涂层的耐腐蚀性和耐磨性能的影响。所用电解液为含有磷酸盐和硅酸盐的碱性溶液,并采用两种不同的PEO处理时间(1min和3min)。用动电位极化法和电化学阻抗谱(EIS)分析涂层的耐腐蚀性,用平面-盘式滑动摩擦实验测试其耐磨性能。用扫描电镜及能谱仪(SEM-EDS)观察涂层的组织形貌、微观结构、元素组成和涂层厚度。结果表明,石墨纳米颗粒增加了涂层的厚度,封闭了表面的孔隙,使涂层更致密,因此提高了其耐腐蚀性和耐磨性能。由于AZ91具有更高的铝含量,其耐腐蚀性能和耐磨性能的提高比AZ80更显著。
简介:Semi-solidAl2Y/AZ91magnesiummatrixcompositesslurrywaspreparedbyultrasonicvibration,effectofultrasonicvibrationtemperatureandtimeonmicrostructureofsemi-solidslurrywasinvestigated.Theresultsshowedthatwiththeultrasonicvibrationtemperaturedecreasingthesolidvolumefractionofsemi-solidslurryincreased.Thebestultrasonicvibrationtemperaturewas600oC.Withtheincreaseofultrasonicvibrationtime,theaveragegraindiameterofprimaryа-Mgparticlesdecreasedfirstly,thenincreased,theaverageshapefactorincreasedgraduallyanddecreasedslightlyafter90s,andafewrosettedendriteswereobservedafter120s.Thebestsemi-solidslurrywithaveragegraindiameterof75μmandshapefactorof0.7weregainedafterthemeltwastreatedbyultrasonicvibrationforabout60satnearliquidustemperature(600oC).Atlast,themicrostructureevolutionmechanismofsemi-solidmagnesiummatrixcompositesslurrywasanalyzedbythetheoriesofthermodynamicsandkinetics.
简介:Arheo-diecastingprocess(RDC)wasinvestigatedforsemisolidprocessingofanAZ91Dmagnesiumalloy.TheresultsoftheRDCsamplesinas-caststateindicatethatthemicrostructureofprimaryα-Mgparticleshasafinesize,nearlysphericalmorphology,anduniformdistributionthroughoutthecomponents.Duetotheadvancedmicrostructureandreducedlevelofdefects,theRDCAZ91DMgalloyexhibitsanapparentimprovementinmechanicalproperties.Thequantitativemetallographicinvestigationsrevealthatincreasingtheintensityofforcedconvectionduringtheslurrypreparationresultsinapromotednucleationandreducedvolumefractionoftheprimaryphasesolidifiedintheslurrymaker.
简介:Energy-storageweldingconnectioncharacteristicsofrapidlysolidifiedAZ91DMgalloyribbonswith40~70μmthicknessareinvestigatedusingamicrotypeenergy-storageweldingmachine.Themicrostructureandperformanceoftheconnectionjointsareanalyzedandstudied.Theresearchresultsindicatethatenergy-storageweldingisabletorealizethespotweldingconnectionofAZ9lDMgalloyribbons.Theweldingnuggetconsistsofdevelopedα-Mgequiaxedgrainswiththesizesof1.2~2.7μmandintergranulardistributedβ-Mg17Al12compounds.Thethicknessofbondzoneisabout4μmandthesolidificationmicrostructureischaracterizedbythefineequiaxedgrainswiththesizesof0.8~1.2μm,andgrainboundaryhasbecomecoarsening.ThecolumnarcrystalinHAZalsobecomesslightlycoarseningandthegrainboundaryhasbroadened,however,thereisnoobviouschangeinitsprimitivemorphologyandcrystallographicdirection.Whenweldingenergyisabout2.0J,theweldingjointswithhighershearstrengthandsmallerelectricalresistivityareobtained.
简介:到改善AZ91D镁合金的bioactivity和腐蚀抵抗,有新奇microstructured形态学的hydroxyapatite(幸运)涂层经由一个灵巧的热水的方法在AZ91D底层上成功地被准备。不同chelating代理人包括polyaspartic酸(PASP)和ethylenediaminetetraacetic酸(EDTA)被介绍在形态学和腐蚀上调查他们的效果涂的镁的抵抗合金。结果表明准备与的涂层PASP是许多一致像顽童的microspheres镇静,当与EDTA准备的涂层由许多象花的粒子组成了时。而且,与EDTA准备的涂层的crystallinity比的高是大部分与PASP准备的涂层。电气化学的测试表明底层的腐蚀抵抗显著地在与每涂层是涂的以后被改进。在模仿的身体液体(SBF)的涂的样品的沉浸测试证明涂层能逐渐地是biodegraded并且导致钙磷酸盐粒子的形成。
简介:thermomechanically影响的地区(TMAZ)的微结构进化特征合金在磨擦期间促使处理(FSP)thixoformed(TF),AZ91D合金被调查。同时,合成的层增强了由的表面原文如此,粒子(SiCps)被FSP在合金上准备,相应tribological性质被检验。试验性的结果显示那动态再结晶和机械分离(包括切开和主要谷物的骨折)是为TMAZ的谷物精炼的主要机制。一致地分布式的SiCps增强的合成表面在合金上被准备。与没有合成表面,扔合金和TF合金的相应永久模子相比,有合成表面的TF合金有最高穿抵抗和最低磨擦系数。
简介:由于人们对锻造镁合金兴趣的增加,所以对锻造镁合金的成形性能进行研究。研究应用了连续铸造再挤压成形的AZ31和AZ80镁合金坯料。由室温下的压缩试验测得所研究坯料的力学性能,还测试了不同热处理的试样。此外,测得了在300~450℃、应变速率ε为1s^-1的条件下单轴平面应变镦粗试验时的真实应力曲线。不同热体积成形条件下试样的真实应力曲线与微观组织的定量分析结果有关。为了确定所应用镁合金的成形性能,采用等温模具进行了体积成形试验。试验用液压锻造压力机的滑块速度为1~40mm/s。所使用的两种镁合金均可生产出形状简单的典型锻件。