简介:Thereactionofsillimanitewithaluminaattemperatures1650℃an1750℃hasbeeninvestigated.Theresultshaveshownthat,inthelaboratorytestconditions,thehigherthealuminacontent,thelowerwillbetheamountsofglass-phseofthefiredbodyandthehigherwillbetheformationofmullite.Inthepresenttests,however,thereactioninconcernhasnotbeencompleted,thereactioninconcernhasnotbeencompleted.Someuncombinedresidualaluminastillexistintheformofcorundum.
简介:Calciumhexaluminate(CA6)wassynthesizedbymixinglight-weightcalciumcarbonateandAl2O3micropowder(calcinedα-Al2O3,activatedα-Al2O3orρ-Al2O3)accordingtothestoichimetricratioofCA6,andreactionsinteringat1200,1300,1400and1500℃for3h,respectively.Effectsofthethreealuminamicropowdersonthephasecomposition,microstructureandpropertiesofCA6wereinvestigated.Theresultsshowthat:(1)forthethreeAl2O3micropowders,thereactiontogenerateCA6inspecimensbasicallycompletesatabout1500℃;CA6generatedinallspecimensisplanar,butthearraymodesareslightlydifferent;(2)thespecimenspreparedfromcalcinedα-Al2O3orρ-Al2O3shrinkalmost,whilethespecimenspreparedfromactivatedα-Al2O3expand;(3)thecoldcrushingstrengthofthespecimenpreparedfromactivatedα-Al2O3isthehighest,reaching42.5MPawhenonlyCA6exists(afterfiringat1500℃);(4)thespecimenpreparedfromρ-Al2O3hasthelowestgenerationtemperatureofCA6andthehighestapparentporosity,reaching70.1%whenonlyCA6exists(afterfiringat1500℃);(5)thespecimenpreparedfromcalcinedα-Al2O3hasthebiggestbulkdensity.
简介:Thedevelopmentandapplicationofdomesticspinelandhigh-alumian/spinel(includingcorun-dum/spinelandcalcined-bauxite/spinel)castablesweredisucssedinthispaper,Itexpoundedthetech-nicalcharactersandvirtuesofhighgradeandmedi-umgradespinelandtheimportanceofthedevelop-metandsuccessfulapplicationofcalcined-bauxite/spinelcastalbes.Becauseofthetechnicalandeco-nomicalfeasibility,thedevelopementandapplicationofspinelandhigh-alumina/spinelcastables,inwhichdomesticrefractoryworkersplayanimportantrole,havebeenflurishing.
简介:Thegrain-growthbehaviorofAl2O3powdercompactswithsmallcontents(<5wt%)ofvariousdopantswasstudied.Theexistenceoftabularsub-grainswereobservedwithallthefollowingdopants:V2O5,MgO+Y2O3andNa2B4O7+V2O3+Pr.Thetabularsubgrainsaredefinedastheabnormalgrainslongerthan30μmwithanaspectratio>50.Theycanbeobservedwhenthesinteringtemperaturearehigherthan1850℃。
简介:Thereproducingalumina-magnesia-carbonbrickswerepreparedwiththedumpedbricksasstartingmaterials.Thebulkdensity,apparentporosity,crushingstrength,modolusofruptureandslagresistanceofthespecimenwereanalyzed.Theresultsshowthattheusedrefractoriescanbereusedandrecycledbytherightmethod.Thereproducingalumina-magnesia-carbonbrickswithbetterabilitieswereprepared.
简介:Inthiswork,therheologicalbehaviorofultra-lowcementalumina-basedcastableswithadditionofflakegraphiteandextrudedgraphitepelletshasbeeninvestigatedbyusingIBBrheometer.Emphasishasbeenlaidontheinfluenceofthetypeandamountofcarbonadditiononrheologicalpropertiesofthealumina-basedcastablesandtheresultsarecomparedwithcorrespondingaluminacastablesampleswithoutanycarbonaddition.Itisfoundthatalumina-basedcastableswithextrudedgraphitepelletshavegoodrheologicalbehaviorandflowabilitywithlowerwaterdemand(<6.3%)andnosegregationduringtheshearingofcastable.
简介:Withtherapiddevelopmentofcomputertechnique,Computeraideddesign(CAD)andcomputeraidedmanufacturing(CAM)orcomputerintegratedmanufacturing(CIM)hasbecameanalternativetotheconventionaltechniqueforproducingdentalrestorations.
简介:ThefracturetoughnessandfractureworkofAl2O3/SiCprismaticceramiccompositeswasevaluatedinthispaper,whichshowedthefractureenergywasimprovedgreatly.Basedontheobservationforcrackpropagationandfracturemorphology,thefracturebehavioroftheprismaticcompositeswasanalyzed.Inthebendingtest,thecompositesdisplayedanon-catastrophicbehaviorandagracefulfailurewithreasonableload-carryingcapability.
简介:Theeffectsofseveralcommercialdispersants,includingAN-2000,ammoniumpolyacrylate,sodiumtripolyphosphate,sodiumhexametaphosphate,andofsolidsloadingandofelectro-fusedmagnesiaonrheologicalpropertiesofaqueousalumina-spinelslurrieswerestudied.TheresultsrevealthatAN-2000isthemosteffectiveoneamongtheselecteddispersantsforalumina-spinelslurries.With0.5%weightofAN-2000,the57vol%solidsloadobtainedatshearrateof50s-1.
简介:Aluminamagnesiacastablecruciblespecimenswerepreparedusingtabularcorundum(≤5mm),fusedmagnesiapowder(≤0.088mm),fusedspinelpowder(≤0.044mm),andα-Al2O3micropowder(d50≤0.7μm)asmainstartingmaterials,batching,mixing,shaping,anddrying.Slagresistancewasdeterminedbystaticcruciblemethodat1600℃for3hadoptingtwoladleslagswithdifferentbasicities(3.40and1.03).Thecorrosionandpenetrationindexesandmicrostructurecharacteristicsofthespecimensafterslagresistancetestwereanalyzedtostudythecorrosionbehaviorsofthetwoslagstoaluminamagnesiacastables.Theresultsshowthatthecorrosionofthelowbasicityslagtoaluminamagnesiacastablesismuchmoreseriousthanthatofthehighbasicityslagforthattheirreactionswithcastablesformdifferentproducts;forthelowbasicityslag,themulti-phasecoexistenceofCA6andcompoundsofCaO-Al2O3-SiO2inthematerialstogetherwithvolumeexpansioncausedbytheformationofCA6intensifytheslagcorrosionandpenetration;forthehighbasicityslag,thereactionbetweenslagandcastablesgeneratesaCA2denselayerandalargeamountofin-situMAintheinterface,reducingtheslagcorrosiontothematerialseffectively.