简介：提出了一种在带有反转平台的精密离心机上标定陀螺加速度计二次项系数丘的方法。阐述了其测试原理，指出这种带反转平台的测试原理改善了PIGA离心机测试的环境条件。所提出的测试方案和辨识方法解决了陀螺加速度计在精密离心机上进行高占测试时，受到离心机大臂旋转牵连运动影响的关键问题，并提出分离和精确标定陀螺加速度计二次非线性项系数届的数据处理方法，解决了反转平台引入后造成的正弦输入问题。

简介：RandomfatigueofweldedK-typetubularjointssubjectedtoaxialorout-of-planebendingloadisanalyzed.Byconsideringthesizesofinitialsurfacecracksandmaterialconstantsasrandomvariableswithsomeprobabilisticdistributions,incorporatingtheeffectoftheweld,fivehundredrandomsamplesaregenerated.Statisticalcomputationalresultsoflifeofcrackpropagationandeffectofchangeofcrackshapearefinallyobtainedandcomparedwithexperimentaldataavailablebasedonaregressionanalysis.Meanwhile,crackpropagationbehaviorsarealsoinvestigated.

简介：K-phillipsite用一个热水的方法被准备。可溶的玻璃和钠铝酸盐当一个器官的模板不在时被用作原料。关于K+离子的调查在房间温度被进行在海水样品和混合K+Na+答案的选择系数决定离子交换能力。样品被X光检查衍射(XRD)描绘，扫描电子显微镜学(SEM)，和精力分散光谱学(版本)。K+离子交换能力是在海水的51mg/g，选择系数在混合K+Na+答案是75.1。样品为K+有选择偏爱，并且能因此被用来有选择地从海水提取钾。由Si，艾尔，K，Na，和O组成的样品展出跨like形状并且是典型K-phillipsite结构。

简介：ThecharacteristicsofsuspendedsedimentimagecanbereflectedbythecoefficientsofbiorthogonalwavelettransformofCDF(2,2).Basedonthepowerdistributionindifferentscales,anadaptivealgorithmisproposedinthispaper,wherebythecoefficientsareadjustednon-linearly.Theparticleinformationcanbewellretainedwhiletheuselessbackgroundisremoved.Inthisway,satisfactorybinaryimagecanbeobtainedforfurtheranalysisofthesedimentparticle.

简介：

简介：TiO2@ZrO2@Y2O3:有coremultishell结构的Eu3+合成粒子通过layer-by-layer(LBL)的联合被综合自己组装方法和一个solgel过程。获得的样品与扫描电子被描绘显微镜学(SEM)，传播电子显微镜学(TEM)，X光检查光电子光谱学(XPS)，X光检查衍射(XRD)，和荧光spectrophotometry。结果证明合成粒子有coremultishell结构，球形的形态学，和狭窄的尺寸分布。TiO2核心上的ZrO2层的存在能有效地阻止在TiO2核心和Y2O3壳之间的反应；为在在TiO2@ZrO2@Y2O3的TiO2核心和Y2O3壳之间的反应的温度:Eucoremultishell黄磷能被300提高

简介：TheinfluenceofNa2SO4ontheformationofZnOwhiskerswasinvestigatedinthispaper.ZnOwhiskerswithaspectratiosofupto50weresynthesizedbydissolvingε-Zn（OH）2precursorinNaOH/Na2SO4solutionatroomtemperature,followedbyagingoftheresultingsolutionat140℃for6h.Fouriertransforminfraredspectroscopy,Ramanspectroscopy,andX-rayphotoelectronspectroscopyanalysesrevealedthatSO42-ionswereprimarilyadsorbedonthe（100）planeoftheZnOwhiskersviaanouter-spherecomplexconfiguration（O-H…O）,therebypromotingtheone-dimensionalgrowthofZnOwhiskersalongthec-axis.

简介：TiO2nanoparticlesweresynthesizedbyahomogeneouscontrolledprecipitationmethodusingindustrialtitaniumsulfate(Ti(SO4)2).TheobtainedpowderswerecharacterizedbyX-raydiffraction(XRD),transmissionelectronmicroscope(TEM),Fouriertransforminfraredspectroscopy(FTIR)andICPplasmaspectrometer.EDTAwasusedascomplexingagenttoimprovethepurityandtheformationofTiO2nanoparticles.Experimentalresultsindicatedthatthehigh-purityTiO2nanoparticleswere20nminmeansizeandnearlymonodispersed.

简介：PureAl2O3-2SiO2powderswerepreparedbysol-gelandcoprecipitationmethods,andtheiralkaliactivationreactivitieswerecompared.Thealkali-activationreactivityofthepowderpreparedbythesol-gelmethodwashigherthanthatofthepowderpreparedbythecoprecipitationmethod.Thepowderswereinvestigatedby27AIand29Simagic-anglespinningnuclearmagneticresonancespectroscopy（MASNMR）tounderstandtherelationshipbetweentheirstructureandalkali-activationreactivity.The27AlMASNMRdatashowedthatthefive-coordinateAIcontentofthepowderpreparedbythesol-gelmethodwashigherthanthatofthepowderpreparedbycoprecipitation.Thehighercontentoffive-coordinateAlcorrespondedtohigheralkali-activationreactivity.The29SiMASNMRdatashowedthatforthepowderpreparedbythesol-gelmethod,siliconwasreplacedbyaluminumatsecondarycoordinationsitesofthecentralSiatomsduringcalcination.However,forthepowderpreparedbysingle-batchcoprecipitation,themainchangewasfromalowdegreeofpolycondensationtoahighdegreeofpolycondensation.

简介：HomogeneousNi2+-dopedtitaniagelwassynthesizedbyasol-gelprocess,andthexerogelwasthenobtainedthroughaginganddrying,leadingtotheformationofNi/TiO2nanocompositeafterheattreatmentunderasuitablereducingatmosphere.TheresultingnanocompositewascharacterizedbyTGA-DSC,TEM,XRDandBETmethods.Theresultsshowthatthestructureandgrainsizeofthenanocompositescouldbemanipulatedbyalteringtheheat-treatmentconditions,andthatthenanocompositepossessesamesoporousstructurewithaporeradiusofca.28nmandaspecifictheanatase-rutilephasetransformation.

简介：DrivenbycuriosityaboutpossibleflightoptionsfortheChang’e-2spacecraftafteritremainsattheSun-EarthL2point,effectiveapproachesweredevelopedfordesigningpreliminaryfuel-optimalnear-Earthasteroidflybytrajectories.Theapproachesincludetheuseofmodifiedunstablemanifolds,gridsearchofthemanifolds’parameters,andatwo-impulsemaneuverfororbitalphasematchingandz-axisbiaschange,andaredemonstratedtobeeffectiveinasteroidtargetscreeningandtrajectoryoptimization.Asteroidflybysareexpectedtobewithinadistanceof2×107kmfromtheEarthowingtotheconstrainedEarth-spacecraftcommunicationrange.Inthiscase,thespacecraft’sorbitalmotionissignificantlyaffectedbythegravitiesofboththeSunandtheEarth,andtherefore,theconceptofthe"heliocentricoscillating-Keplerorbit"isproposed,becausetheclassicalorbitalelementsoftheflybytrajectoriesreferencedintheheliocentricinertialframeoscillatesignificantlywithrespecttotime.Theanalysisandresultspresentedinthisstudyshowthat,amongtheasteroidswhoseorbitsarethemostaccuratelypredicted,"Toutatis","2005NZ6",or"2010CL19"mightbeencounteredbyChang’e-2inlate2012or2013withtotalimpulseslessthan100m/s.

简介：惯性平台安装在舰船的过程中需要将惯性平台坐标系与舰船坐标系进行对准，也就是对惯性平台进行标校。当舰船在倾斜船台上进行建造时，由船台的倾斜角度造成水平测量仪器的测量误差对标校的结果有很大影响，尤其是在测量舰船横摇角时，会由于测量仪器的摆放带来误差。船台的倾斜角度为3°时，边长为100mm的水平测量仪器在测量横摇角时产生0.1°的测量方位误差（即水平测量仪器一端产生0.17mm位移），就会带来18.8″的测量误差。这对于高精度惯性平台的标校是不允许的。文中对在各种不同舰船姿态下，由测量仪器的摆放带来的误差进行了分析归纳。利用双自由度电子水平仪、高精度转台及TM5100A自准直经纬仪，对由于安装面倾斜带来的测量误差进行了验证试验。实验结果与计算结果吻合。

简介：Lithium-aluminum-cobalt-nickeloxideLiAlxCoyNi1xyO2particles,generallyusedascathodeoflithiumbattery,werepreparedbychemicalcoprecipitationfromanaqueoussolutionofLiOH,Al(NO3)3,Co(NO3)2andNi(NO3)2withNH4OH.XRD,SEMandFTIRwereusedtoexaminetheeffectofnickelcontentontheproduct.FTIRpatternsshowedthatincreaseinnickelcontentdecreasedtheabsorptionstrengthofthepeakofspinelstructureoftheproduct,attributedtotheoccupationbynickelinthealuminumsites.Particlesizeandelectricalpropertiesofthelithium-aluminum-cobalt-nickeloxide(abbreviatedasLACNO)particleswerealsodetermined.

简介：The(2+1)-dimensionalBKPequationintheHirotabilinearformisstudiedduringthiswork.WronskianandGrammiantechniquesareappliedtotheconstructionofWronskianandGrammiansolutionsofthisequation,respectively.ItisshownthatthesesolutionscanbeexpressedasnotonlyPfaffiansbutalsoWronskiansandGrammians.

简介：

简介：水平姿态误差标定是提高测量船惯性导航系统精度的重要手段。传统的水平精度标定一般只能在实验室或坞内等静态条件下通过高精度水平仪来实现。针对动态条件下水平作差、平台旋转及经纬仪方位俯仰信息联立求解等标定方法存在标定条件苛刻、精度相对较低等局限性,提出了一种基于星体测量的惯导水平姿态标定新技术——俯仰脱靶量求解法,推导了计算公式,并对解算精度进行了系统分析。通过惯导精度鉴定及某次试验任务的检验,其解算精度在5.8″以内,具有较高的置信度。该方法解决了惯导水平姿态动态条件下标定的技术难题,为提高惯导水平姿态精度、实战数据的事后处理以及动态条件下加速度计零位标定提供了依据,对提高航天测量船总体测量精度具有重要意义。

简介：Thecoordinationpolymer,(Nd(H2O)5)2(2,6-AQDS)3·2H2Owhere2,6-AQDS=2,6-anthraquinonedisulfonate,hasbeensynthesisedviaahydrothermalroute.Structurally,itconsistsoflayersofmonomericNdpolyhedrawhicharelinkedby2,6-AQDSanionsformingapolymeric,three-dimensionalnetwork.EachNdatomisninecoordinate,bondingtofivewatermoleculesandtofouroxygenatomsfromfour2,6-AQDSanionswhichinturnpillarthelayersbybridgingtwoNdatomsinonelayer,andcoordinatingtoasingleNdintheother.

简介：NanocrystallineSnO2wassynthesizedbydirectmixingandgrindingofSnCI4-5H2OandNaOHatroomtemperature,followedbycalcinationatdifferenttemperaturesfordifferenttimesinair.ProductsampleswerecharacterizedbyX-raydiffractionandtransmissionelectronmicroscope,revealingthattheamorphousprecursorSnO2wastransformedtocrystalsat200℃for3h,andthattheaverageparticlesizeincreaseduponraisingthecalciningtemperatureorprolongingthecalciningtime.Themechanismofthephasetransformationoftheproductsisdiscussed.

简介：连贯的多角形的粒子的二维的分离元素模型(DEM)模拟被开发了估计点来源颤动的利益在楔形的hoppers导致流动。使用的particleparticle相互作用模型基于一个多接触原则。没有颤动，学习的第一部分在严肃下面调查了粒子分泌物决定批评的孔尺寸(Bc)就作为粒子形状的功能支撑流动。多角形形状的粒子比圆形的粒子需要一个更大的孔，这被显示出。当粒子顶点的数字增加，Bc减少，这也被显示出当粒子顶点的数字增加。圆形的粒子的增加以一种线性方式支持多角形的流动。学习的第二部分证明那颤动能提高流动，有效地减少Bc。模型表明了震荡器地点(高度)的重要性，与在提高的以前的连续统模型结果，和颤动振幅一致流动。

简介：Uniformlysizedα-Fe2O3hexagonalplateletsweresynthesizedbyahydrothermalprocessusingFe(OH)3suspensionandlargeamountofNaOH.ThereactionproductswerecharacterizedbyX-raydiffraction(XRD),scanningelectronmicroscopy(SEM),transmissionelectronmicroscopy(TEM),selectedareaelectrondiffraction(SAED),andavibratingsamplemagnetometer(VSM).Theresultsshowthatthehexagonalplateletsarefine,monodisperseandconsistingofsingle-crystals.Themagnetichysteresis(M-H)curveofthesamplesmeasuredatroomtemperatureindicatesthattheα-Fe2O3micro-plateletsexhibitferromagneticbehaviorswithrelativelylowcoercivity.