PREPARATION AND MICROSTRUCTURE CHARACTERIZATION OF Ni／TiO2 NANOCOMPOSITE-中国期刊网

摘要 HomogeneousNi2+-dopedtitaniagelwassynthesizedbyasol-gelprocess,andthexerogelwasthenobtainedthroughaginganddrying,leadingtotheformationofNi/TiO2nanocompositeafterheattreatmentunderasuitablereducingatmosphere.TheresultingnanocompositewascharacterizedbyTGA-DSC,TEM,XRDandBETmethods.Theresultsshowthatthestructureandgrainsizeofthenanocompositescouldbemanipulatedbyalteringtheheat-treatmentconditions,andthatthenanocompositepossessesamesoporousstructurewithaporeradiusofca.28nmandaspecifictheanatase-rutilephasetransformation.

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PREPARATION AND MICROSTRUCTURE CHARACTERIZATION OF Ni／TiO2 NANOCOMPOSITE

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PREPARATION AND MICROSTRUCTURE CHARACTERIZATION OF Ni／TiO2 NANOCOMPOSITE

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