Aneficientliquid-phasesynthesisofisoxazolinesthrougha1,3-dipolarcycloadditionisdescribed.Solublepolymer-supportedacrylatereactedwithnitrileoxidesgeneratedin-situ,followedbycleavagefromthesupportgivingcorrespondingisoxazolinesinhighyieldsandexcellentpurities.