简介:Commerciallyavailablelatticescontainvariouskindsofmorphologicalimperfectionswhichresultingreatdegradationinlattices’mechanicalproperties,therefore,toobtainimperfectioninsensitivelatticestructureisobviouslyapracticalresearchsubject.Hierarchicalstructurematerialswerefoundtobeaclassofpromisinganti-defectmaterials.Thispaperbuildshierarchicallatticebyaddingsoftadhesiontolattice’scelledgesandnumericalresultsshowthatitsimperfectionsensitivitytomissingbarsisminorcomparedwiththeclassiclattice.Softadhesionwithappropriatepropertiesreinforcecelledge’sbendingstiffnessandthusreducethebendingdeformationinlatticecausedbymissingbarsdefect,whichisconfirmedbystatisticalanalysisofnormalizednodedisplacementsofimperfectlatticesunderhydrostaticcompressionandshearloads.
简介:Inthisarticle,low-pressurecontrolmethodsforacombinedarcsubmergednanoparticlesynthesissystem(ASNSS)wasproposedanddevelopedforTiO2nanoparticlefabrication.Thephotocatalyticreactioniscarriedoutinaphotochemicalreactor.TheUVlightisobtainedfromUV-lampswithwavelengthof(253.7±0.8)nm.TheUV-Visspectrometryisusedtomonitortheabsorbancespectraofmethyleneblueasafunctionofilluminationtime.ExperimentalresultsshowthattherateconstantofphotocatalyticreactionofTiO2nanoparticlesformethyleneblueis0.0365min^-1.Thesurfaceadsorptionplaysanimportantroleinthedecompositionofmethyleneblue.ExperimentalresultsindicatethattheTiO2nanoparticlefluidpossessesexcellentphotocatalyticactivityinphotodegradationofmethyleneblue.
简介:为了提高标准Cubature卡尔曼滤波(CKF)的稳定性和鲁棒性,提出一种改进的多重渐消H∞滤波cubamre卡尔曼滤波算法。首先基于系统状态的可观测性给出多重渐消因子矩阵求解过程,提高滤波算法的稳定性,抑制滤波发散;其次,引入H∞鲁棒思想,构造多重渐消H∞滤波Cubature卡尔曼滤波器;最后,提出采用一种奇异值分解的矩阵分解策略代替标准Cubature卡尔曼滤波中的Cholesky分解,进一步提高算法的数值稳定性。实际GPS/INS组合导航实验表明,改进的多重渐消H∞滤波Cubature卡尔曼滤波算法不仅能有效抑制滤波发散提高算法的稳定性,而且对观测野值具有更高的鲁棒性;提出的新算法与标准CKF算法相比,XYZ三个方向的位置精度分别提高了55.8%,46.6%和39.7%。
简介:Thereisaneedtostandardizemethodsassociatedwiththedispersionofnanomaterialsinnano(eco)toxicologicalinvestigations.Thefirststeptowardthisgoalistounderstandthedegreeofvariabilitythatexistsinnanomaterialdispersionspreparedbyusingdifferentprotocols.Usingtwocasestudies,thedegreeofvariabilityinTiO2nanomaterialdispersionswasassessedbydifferentialcentrifugalsedimentation(DCS)methods.Casestudy1addressesthevariabilitythatarisesfromvariationswithinoneprotocol,investigatingtheeffectsofdispersionaging,sonicationexposuretime,sonicationinthepresence/absenceofanicebath,materialsubsampling,particleconcentrationandhavingapre-wettingstep.Casestudy2addressesthevariabilitybetweenfourdifferentprotocolsdevelopedthroughpastresearchactivitiesandprojects.Theresultsindicatethatthereisalargedegreeofvariability(relativestandarddeviation(RSD)ofmeanparticlediameter=26%)inthedispersionofTiO2nanomaterialsbetweenthefourdifferentprotocolsstudiedandthatseveralstepsinadispersionprotocolarepotentialsourcesofvariation,withfinalparticleconcentrationbeingthemostsignificant.Theimplicationofthisstudyisclear:forthepurposeofdatacomparability,thereisaneedtoprovidetheexactdetailsofallstepsinvolvedinadispersionprotocol.
简介:Laminatedcompositematerialsarewidelyimplementedinseveralengineeringconstructions.Foritsrelativelightweight,thesematerialsaresuitableforaerospace,military,marine,andautomotivestructuralapplications.Toobtainsafeandeconomicalstructures,themodellinganalysisaccuracyishighlyrelevant.Sincemeshlessmethodsintherecentyearsachievedaremarkableprogressincomputationalmechanics,thepresentworkusesoneofthemostflexibleandstableinterpolationmeshlesstechniqueavailableintheliterature—theRadialPointInterpolationMethod(RPIM).Here,a2Dapproachisconsideredtonumericallyanalysecompositelaminatedbeams.Boththemeshlessformulationandtheequilibriumequationsrulingthestudiedphysicalphenomenonarepresentedwithdetail.Severalbenchmarkbeamexamplesarestudiedandtheresultsarecomparedwithexactsolutionsavailableintheliteratureandtheresultsobtainedfromacommercialfiniteelementsoftware.Theresultsshowtheefficiencyandaccuracyoftheproposednumerictechnique.
简介:ThecaptureoforthophosphatesandtotalphosphorusfromthePudongCanalriverinthePudongDistrictofShanghaibyTiO2nanoparticlesisstudiedusingarotatingphotoreactorandthenano-TiO2photocatalystDegussaP25.TheeffectsofUVirradiationintensityinarangeof20-74mW/cm2.theloadingoftheTiO2nanoparticlesinarangeof0.05-0.1g/L,irradiationtimeupto4h,andpHvaluesinarangeof2-10.5onthecaptureefficiencyareinvestigated.TheresultsshowthatthecaptureoforthophosphatesandtotalParesignificantlyenhancedbyUVirradiation;ataloadingof0.1g/Landanirradiationintensityabove36mW/cm2,orthophosphatesandtotalphosphorusarerapidlycapturedbyTiO2nanoparticles,causinganobservedreductionfrom0.4mg/Ldownto0.02mg/L.pHvaluesinarangeof2-10.5havelittleeffectonthecaptureefficiencyoforthophosphatesandtotalphosphorus.
简介:Hierarchicalsea-urchin-shapedmanganeseoxidemicrospheresweresynthesizedviaatacilemetnoabasedonthereactionbetweenKMnO4andMnSO4inHNO3solutionat50C.Theaveragediameterofthemicrospheresis850nm.Themicrospheresconsistofacoreofdiameterof800nmandnanorodsofwidth50nm.Thenanorodsexistattheedgeofthecore.TheBrunauer-Emmett-Tellersurfaceareaofthesea-urchin-shapedmicrospheresis259.4m2/g.Apossibleformationmechanismofthehierarchicalsea-urchin-shapedmicrospheresisproposed.Thetemperaturefor90%conversionofbenzene(T90%)onthehierarchicalurchin-shapedMnO2microspheresisabout218℃.
简介:ZrO2nanopowdersbasedstearicacidphasechangematerials(PCMs)werepreparedbyhigh-energymilling.Theconceptofheatcapacityfactor(HCF)wasusedtoanalyzethethermalpropertiesofthematerials.TheheatstoragepropertyofPCMs,containingthesamecontentofstearicacid(23%bymass)inthestartingmaterialsbutsynthesizedbydifferenttechnicalprocesses,wasinvestigatedbyusingHCF.Itwasfoundthattherewerevastinfluencesofdifferentdispersantsontheheatcapacity.Thesamplespreparedwithchloroformprovidedthebestheatstorageabilityinallsamplestested.
简介:多路径误差是北斗导航定位系统高精度动态监测的主要误差源。针对北斗导航定位系统多路径误差的特性,结合广义特征值盲源分离方法的优势,提出一种基于参考信号的广义特征值盲源分离算法来削弱多路径效应的影响。首先将前一天的原始坐标残差序列通过奇异谱分析方法进行去噪,其结果作为初始参考信号;然后将当天的原始坐标残差序列进行经验模式分解方法分解,分解得到的IMF分量作为虚拟观测数据,利用广义特征值盲源分离算法获取当天多路径误差信号;最后,利用仿真数据和连续10天的实际观测数据进行试验分析,结果表明利用该方法建立的多路径误差改正模型能有效地了削弱多路径的影响,北、东、天三个方向精度分别提高了78.8%、35.3%、90.1%。提出的模型在一定程度上解决了固定多路径模型随着时间推移重复性减小且有效性降低的问题。
简介:Anewmicromechanicsconstitutivemodelforpuredilatanttransformationplasticityofstructureceramicsisproposedinthispaper.Basedonthethermodynamics,micromechanicsandmicroscalet→mtrans-formationmechanismanalysisoftheTZPandPSZZrO2-containingceramics,ananalyticexpressionsoftheHelmholtzandcomplementaryfreeenergyoftheconstitutiveelementforthecaseofpuredilatanttransforma-tionisderivedforthefirsttimeinaself-consistentmanner.Bytheanalysisofenergydissipationinthefor-wardandreversetransformations,themieromechanicsconstitutivelawisderivedintheframeworkofHill-Rice’sinternalvariableconstitutivetheory.
简介:Afacilemethodforthesynthesisofsilver-silica(Ag-SiO2)Janusparticleswithfunctionalitiessuitablefortextileapplicationsisreported.SilicananoparticlespreparedbytheStobermethodwerefunctionalizedwithepoxy,amine,andthiolgroups,whichwereconfirmedbyFouriertransforminfraredanalysis.ThefunctionalizedsilicananoparticleswereusedtoproducePickeringemulsions,andtheexposedsurfacewasusedfortheattachmentofsilvernanoparticles(AgNPs)viathelow-temperaturechemicalreductionmethod.ThemorphologyandstructureoftheAg-SiO2Janusparticleswerecharacterizedbyscanningelectronmicroscopy,scanningtransmissionelectronmicroscopy,high-resolutiontransmissionelectronmicroscopy,energy-dispersiveX-rayanalysis,andUV-visspectroscopy.Becauseoftheirspecificfunctionalities,theseAg-SiO2Janusparticlesareproposedforapplicationsontextilesubstrates,astheycanovercomeseveraldrawbacksofdirectapplicationofAgNPsontextiles,suchasleaching,agglomeration,andinstabilityduringstorage.
简介:Thispaperpresentsanovelmechanicalattachment,i.e.,nonlinearenergysink(NES),forsuppressingthelimitcycleoscillation(LCO)ofanairfoil.Thedynamicresponsesofatwo-degree-of-freedom(2-DOF)airfoilcoupledwithanNESarestudiedwiththeharmonicbalancemethod.DiferentstructureparametersoftheNES,i.e.,massratiobetweentheNESandairfoil,NESofset,NESdamping,andnonlinearstifnessintheNES,arechosenforstudyingtheefectoftheLCOsuppressiononanaeroelasticsystemwithasupercriticalHopfbifurcationorsubcriticalHopfbifurcation,respectively.TheresultsshowthatthestructuralparametersoftheNEShavediferentinfluenceonthesupercriticalHopfbifurcationsystemandthesubcriticalHopfbifurcationsystem.
简介:为它的高氧化抵抗,钇硅酸盐是为在在1600°C上面的温度的carbon-fiber-reinforcedcomposites的保护的涂层的一个重要候选人。一个新奇方法,由一起沉淀组成,弄干水花,热处理和plasma-densification,被开发准备Y2SiO5粉末为热喷洒。作文,形态学和综合Y2SiO5粉末的流动能力被XRD,SEM和霍尔流量计分别地调查。结果证明综合Y2SiO5粉末与高纯净是将近球形的。分别地,Y2SiO5粉末的明显的密度和流动能力是1.87g/cm3和37s/50g它为大气的血浆喷洒导致多达80%的高免职效率。
简介:Aunifiedperturbationtheoryisdevelopedhereforcalculatingsolitarywavesofallheightsbyseriesexpansionofbaseflowvariablesinpowersofasmallbaseparametertoeighteenthorderfortheone-parameterfamilyofsolutionsinexactform,withallthecoefficientsdeterminedinrationalnumbers.Comparativestudiesarepursuedtoinvestigatetheeffectsduetochangesofbaseparameterson(i)theaccuracyofthetheoreticallypredictedwavepropertiesand(ii)therateofconvergenceofperturbationexpansion.Twoimportantresultsarefoundbycomparisonsbetweenthetheoreticalpredictionsbasedonasetofparametersseparatelyadoptedforexpansioninturn.First,theaccuracyandtheconvergenceoftheperturbationexpansions,appraisedversustheexactsolutionprovidedbyanearlierpaper[1]asthestandardreference,arefoundtodepend,quitesensitively,onchangesinbaseparameter.Theresultingvariationsinthesolutionarephysicallydisplayedinvariouswavepropertieswithdifferencesfounddependentonwhichproperty(e.g.thewaveamplitude,speed,itsprofile,excessmass,momentum,andenergy),onwhatrangeinvalueofthebase,andontherankoftheordernintheexpansionbeingaddressed.Secondly,regardingconvergence,thepresentperturbationseriesisfounddefinitelyasymptoticinnature,withtherelativeerrorδ(n)(therelativemean-squaredifferencebetweensuccessiveordersnofwaveelevations)reachingaminimum,δm,ataspecificorder,n=nm,bothdependingonthebaseadopted,e.g.n=11-12basedonparameterα(waveamplitude),nm,β=15onβ(amplitude-speedsquareratio),andnm.∈=17on∈(wavenumbersquared).Theasymptoticrangeisbroughttocompletionbythehighestorderofn=18reachedinthiswork.
简介:Nano-sizedhexagonalmagnesiumhydroxide(Mg(OH)2)withgooddispersibilitywassynthesizedbyadoubleinjection-hydrothermalmethod,utilizingpolyvinylpyrrolidone(PVP)asanadditiveandwithoptimizedprocessingparameters.SEMandBETanalysisshowedthatthemeanparticlesizeandspecificsurfaceareaoftheMg(OH)2particleswere174nmand50.77m2/g,respectively.TheFT-IRspectraandtheXRDpatternsshowedthatPVPwasadsorbedonthesurfaceoftheMg(OH)2crystal,thuseffectivelylimitingparticleagglomerationandhinderingcrystalgrowthalongthe(101)plane.TGAshowedadecreaseinthedecompositiontemperatureandanincreaseintheweightlossoftheMg(OH)2particlesduetoadditionofPVP.
简介:从理论上推导了声学超表面对平面声波的作用模型,该理论模型计及声波高阶衍射模态,从而能够计及超表面微结构之间的声学干扰.通过与数值结果对比,该模型预测的反射频率精度得到了一定程度的提高,并能够分辨出相邻孔声场之间的耦合模态.讨论了声学超表面吸声特性与阻抗特性对高超声速边界层内Mack第2模态的抑制机理,研究发现通过设计超表面阻抗特性,使得入射声波与反射声波在壁面处相位相反,同样可以抑制Mack第2模态.基于理论模型,分别优化设计得到最优的微结构几何尺寸,并通过对Mach6平板边界层流动进行稳定性分析,验证了超表面不同声学特性的抑制效果.