简介:AhighlyTm-dopedleadgermanateglassfiberisdevelopedusingtherod-in-tubemethod.The~2μmlaserbeamqualityofthefiberis~1.5.Theleadgermanatecompositefiberjumpersarehomemadeforallthefiberlaserinvestigations.Whencoreispumpedbya1590nmYb/Erfiberlaser,amaximumlaseroutputof313mWisachievedata670mWpumppower,andthecorrespondingslopeefficiencyis~52.8%.Moreover,byusinga2cmlongleadgermanatefiberasthegainmedium,a33mW1942nmTmlaserisalsodemonstrated.
简介:本文报告了应用毛细管气相色谱-质谱(CGC—MS)和傅立叶变换红外光谱(FTIR)联用技术对临床上3起服用毒物自杀的中毒患者尿、胃内容物等样品进行了分析鉴定。样品经酸化和碱化、乙醚抽取,油状物样品用甲醇溶解稀释,然后进行CGC—MS分析。固体样品用氯仿反复洗涤后烘干,KBr压片做FTIR分析。结果检出和确证了患者服用的毒物分别为敌敌畏加糖、速可眠加鲁米那和鲁米那加安定。本法简便、快速、准确,为医院临床抢救提供了可靠的依据。