简介:InordertoobtainultrafineNd-Fe-Bpowder,aspray-driedprecursorwastreatedbyreduction-diffusion(R/D)process.And,unliketheconventionalR/Dprocess,calciumreductionthatisacrucialstepfortheformationofNd2Fe14BwasperformedwithoutconglomeratingtheprecursorwithCapowder.Byadoptingthismodifiedprocess,itispossibletosynthesizethehardmagneticNd2Fe14Batthereactiontemperatureaslowas850℃.TheaveragesizeofNd2Fe14Bparticlesthatareuniformlydistributedintheoptimallytreatedpowderwas<<1μm.MostNd2Fe14BparticleswereenclosedwiththinlayersofNd-richphase.TypicalmagneticpropertiesofsuchpowderwithouteliminatingimpurityCaOwereiHc=~5.9kOe,Br=~5.5kG,and(BH)max=~6MGOe.
简介:Widegapbrazing(WGB)experimentsusingthebuttedspecimenwitha1.5mmgapwerecarriedoutfortherepairofthefailedK418Bsuperalloylow-pressureturbinevanes.Thehightemperaturecreeprupturestrengthsofthebrazedjointsweretested,andthemicrostructuresandfracturesurfacesofthejointswereobserved.TheresultsshowthatthemicrostructureofK418Balloyjointiscomposedofdenseequiaxedgrain,smallanddiscretecompoundswithafewmicro-pores.Duringthecreeprupturetest,thecracksinitiatepreferentiallyatthemicro-poreorthegrainboundary,thenpropagatealongthegrainboundarytillthefracturehappens.Thecreeprupturestrengthat700℃ofthebrazedjointswith50%brazemetalintheworkingpartcouldexceed90%thatoftheK418Bsuperalloy,andthejointswith100%brazemetalintheworkingpartachieve70%to80%ofthecreeprupturestrengthsfortheK418Bbasemetal.