简介:一部新奇二阶段的合成电影被作为陶器的filler作为聚合物矩阵和铋铁酸盐(BFO)扔poly采用的方法(甲基methacrylate)(PMMA)的溶剂准备。BFO的表面是由合适的hydroxylating代理人的functionalized激活他们的化学性质。合成电影的结构的分析证实由functionalizedBFO组成的composites(BFO--哦)有弄歪的菱形的结构。词法分析显示出那BFO--哦粒子同等地在聚合物矩阵上被散布。BFO的-OH功能--哦被FTIR证实。在到1MHz的从100Hz的一个频率范围的绝缘、电的研究揭示那PMMA-(BFO--哦)composites提高了绝缘的经常以及电的传导性,比未修改的composites的高得多。根据铁电体测量结果,hydroxylated合成电影比未修改的的显示出优异铁电体行为,与残余的极化(2P2.764C/cm2的r)。
简介:钡铁酸盐micro/nano纤维成功地经由由把dimethylformamide(DMF)用作溶剂的静电的旋转被准备,并且poly乙烯基pyrrolidone(PVP)作为旋转auxiliaries。结构,形态学,和磁性上的锶替换的效果被扫描电子调查显微镜(SEM),X光检查衍射分析(XRD),和颤动取样磁强计(VSM)。样品的XRD模式证实纯钡铁酸盐纤维形式,和Sr替换做主要山峰(110),(107),并且(114)稍微搬到右。另外,FE-SEM图象证明代替的纤维能保留的Sr完成含纤维的形态学。而且,当纤维在800点被锻烧时,VSM结果证明浸透磁化能到达56.7emu/g'
简介:(Ni0.81Fe0.19)0.66Cr0.34hasahighresistivityandacrystalstructureclosetothatofNi0.81Fe0.19.TheelectricalandX-raydiffractionmeasurementsprovethatathinNiFeCrseedlayerinducesawell(111)-orientedNi0.81Fe0.19film.Post-annealingtreatmentimprovesthemagneticpropertiesof(Ni0.81Fe0.19)0.66Cr0.34(45A)/Ni0.81Fe0.19(150A)/Ta(55A)thinfilmpreparedunderadepositionfield,whereastheinter-diffu-sionofNiFe/Tadeterioratesthemagnetoresistancepropertiesofthefilm.
简介:ThecompositenanofibersofSrTiO3/SrFe12O19withamolarratioof1:1anddiameterabout120nmwerepreparedbyelectrospinning.Effectsofcalcinationtemperatureontheformation,crystallitesize,morphologyandmagneticpropertywerestudiedbyinfraredspectroscopy,X-raydiffraction,scanningelectronmicroscopyandvibratingsamplemagnetometer.Thebinaryphaseofstrontiumferriteandtitanatewasformedafterbeingcalcinedat900℃for2handthecompositenanofiberswerefabricatedfromnanograinsofSrTiO3about24nmandSrFe12O19around33nm.ThecrystallitesizesforthenanofibersincreasewithincreasingcalcinationtemperatureandtheadditionofSrTiO3hasanobvioussuppressioneffectonSrFe12O19graingrowth.Thespecificsaturationmagnetizationandremanencetendtoincreasewiththecrystallitesize.Withincreasingcalcinationtemperaturefrom900to1050℃,thecoercivityincreasesinitially,achievingamaximumvalueof520.2kA·m-1at950℃,andthenshowsareductiontendency.