简介:
简介:BSTOdielectricceramicwaspreparedfromSrTiO3andBaTiO3powderssynthesizedbyhydrothermalmethod,aswellasfromBa0.6Sr0.4TiO3powdersynthesizedbyconventionalsolid-statereaction.Theformercanbesinteredatarelativelylowtemperatureof1120℃.CharacterizationbySEMshowedthatthegrainshapesofbothceramicsarecubical,thoughthegrainsizeoftheformerismuchsmaller.Dielectricconstantsmeasuredat20℃wereshowntovarywithfrequencyintherangefrom1kHzto2MHzanddcbiasfield,andfurtherthatthedielectriclossoftheformertobelessthan2×10-3inthefrequencyrangeof20kHzto1MHz,muchsmallerthanthatofthelattersample.Fortheformer,temperaturedependenceofdielectricconstantismuchflatterandthereexistsanextendedphasetransitiondiffusioncoveringawidetemperaturerangeofCurietemperatureTc.Thesmallergrainsizeoftheformerdepressesthedcbiaselectricalfielddependenceofdielectricconstant.Thetunabilityis7%underabiasfieldof0.6kV/mmdc.
简介:Dispersionofmulti-walledcarbonnanotubesinpoly(p-phenylene)compositeexposedtotoluenewasexperimentallyinvestigated.3mgofmulti-walledcarbonnanotubeswithnominalsizeof20nmwascompoundedwith30mgofpoly(p-phenylene)withthepresenceofterpineolasbindinginitiator.Toinvestigateanoptimalconditionforhomogenizingallconstituents,ultrasonicationwithanoutputpowerof750Wwasemployedwithcompoundingtimeof3,10,20and30min.WithFTIRanalyses,itcouldbeconfirmedthathomogeneouscompositeofmulti-walledcarbonnanotubesandpoly(p-phenylene)couldbeprepared.SEManalyseswerealsoconductedtoexaminethedispersionofmulti-walledcarbonnanotubesinthepolymermatrix.Thenintrinsicelectricalresistanceofthecompositesafterbeingexposedtotoluenewasalsoinvestigated.Itwasfoundthatthecompositefilmpreparedwithultrasonicationfor20mincouldprovidesufficientlysensitiveresponsewithrespecttovariedconcentrationoftoluene.
简介:TiO2@ZrO2@Y2O3:有coremultishell结构的Eu3+合成粒子通过layer-by-layer(LBL)的联合被综合自己组装方法和一个solgel过程。获得的样品与扫描电子被描绘显微镜学(SEM),传播电子显微镜学(TEM),X光检查光电子光谱学(XPS),X光检查衍射(XRD),和荧光spectrophotometry。结果证明合成粒子有coremultishell结构,球形的形态学,和狭窄的尺寸分布。TiO2核心上的ZrO2层的存在能有效地阻止在TiO2核心和Y2O3壳之间的反应;为在在TiO2@ZrO2@Y2O3的TiO2核心和Y2O3壳之间的反应的温度:Eucoremultishell黄磷能被300提高
简介:A3-DnonlinearproblemofsupercavitatingflowpastanaxisymmetricbodyatasmallangleofattackisinvestigatedbymeansoftheperturbationmethodandFourier-cosine-expansionmethod.Thefirstthreeorderperturbationequationsarederivedindetailandsolvednumericallyusingtheboundaryintegralequationmethodanditerativetechniques.Computationalresultsofthehydrodynamiccharacteristicsandcavityshapesofeachorderarepresentedfornonaxisymmetricsupercavitatingflowpastconeswithvariousapex-anglesatdiffer-entcavitationnumbers.Thenumericalresultsarefoundingoodagreementwithexperimentaldata.
简介:Soilconsolidationwouldinducevariationsofitstransportcoefficientssuchashydraulicconductivityanddiffusioncoefficient.Thispaperpresentsastudyoftheinfluenceofbarrierconsolidationontransportcoefficients,anda3Dtransportmodelbasedonmixturetheoryisproposedfordescribingthelinersthatinvolvecirculardefectsinthegeomembrane.TheelastoplasticALPHAmodelisrevisedbyusingthespatiallymobilizedplane(SMP)criterionforsimulatingthedeformationofthesoils.Then,the3Dmodelcouplingthenonlinearconsolidationandcontaminantadvection-diffusionissolvedusingthefiniteelementsoftwareABAQUS.Theresultsshowthattheimportanceofreducingthedefectsizeinthegeomembraneandthelinerporositytocontrolthecontaminantconcentrationincrease.
简介:TheIsodynetechniquebasedonthescatteredlightscanningfromathinlaserbeamcanbeusedtoobtaintheinformationinsidetheloadedobjectintheroomtemperaturenondestructively,soitisaverypowerfultechniquein3Dstressanalysis.Theproblemsarehowtointerprettheinformationandhowtogetsufficientinformationfromthefewinterferencefringe.Birefringencephaseshifttechniquecandistinguishthefringeordersautomaticallyandenrichtheinformationin256graylevelsbetweenmaximandminimlightintensity.InthepapertheIsodynebirefringencephaseshiftmethodwithanobliqueincidenceandequilibriumequationispresented,bywhichthe3DstressesinthemiddleplaneofaplatewithUshapenotchareseparatedsuccessfully.
简介:Basedonthegeneralconservationlawsincontinuummechanics,theEulerianandLagrangiandescriptionsofthejumpconditionsofshockwavesin3-dimensionalsolidswerepresentedrespectively.Theimplicationofthejumpconditionsandtheirrelationsbetweeneachother,particularlytherelationbetweenthemassconservationandthedisplacementcontinuity,werediscussed.Meanwhiletheshockwaveresponsecurvesin3-dimensionalsolids,i.e.theHugoniotcurveswereanalysed,whichprovidethefoundationforstudyingthecouplingeffectsofshockwavesin3-dimensionalsolids.
简介:The1/3subharmonicsolutionfortheDuffing'sequationisinvestigatedbyusingthemethodsofharmonicbalanceandnumericalintegration.Thesensitivityofparametervariationforthetransientprocessandthetransientprocessfortheperturbanceinitialconditionsarestudied.Overandabove,theprecisionofnumericalintegrationmethodisdiscussedandthenumericalintegrationmethodiscomparedwiththeharmonicbalancemethod.Finally,asymptoticalstabilityofthepuresubharmonicoscillationselementisinspected.
简介:Uniformlysizedα-Fe2O3hexagonalplateletsweresynthesizedbyahydrothermalprocessusingFe(OH)3suspensionandlargeamountofNaOH.ThereactionproductswerecharacterizedbyX-raydiffraction(XRD),scanningelectronmicroscopy(SEM),transmissionelectronmicroscopy(TEM),selectedareaelectrondiffraction(SAED),andavibratingsamplemagnetometer(VSM).Theresultsshowthatthehexagonalplateletsarefine,monodisperseandconsistingofsingle-crystals.Themagnetichysteresis(M-H)curveofthesamplesmeasuredatroomtemperatureindicatesthattheα-Fe2O3micro-plateletsexhibitferromagneticbehaviorswithrelativelylowcoercivity.
简介:Becausemostpiezoelectricdeviceshaveinterfaceswithfluidinengineering,itisvaluabletostudythecoupledfieldbetweenfluidandpiezoelectricmedia.Asthefundamentalproblem,the3DGreen'sfunctionsforpointforcesandpointchargeloadedinthefluidandpiezoelectricbimaterialsarestudiedinthispaper.Basedonthe3Dgeneralsolutionsexpressedbyharmonicfunctions,weconstructedthesuitableharmonicfunctionswithundeterminedconstantsatfirst.Then,thecouplefieldinthefluidandpiezoelectricbimaterialscanbederivedbysubstitutionofharmonicfunctionsintogeneralsolutions.Theseconstantscanbeobtainedbyvirtueofthecompatibility,boundary,andequilibriumconditions.Atlast,thecharacteristicsoftheelectromechanicalcoupledfieldsareshownbynumericalresults.
简介:Thisletterobtainsatyphoon-likevortexsolutionbysolvingtheBragg-Hawthorneequation.ThesolutiondescribesspiralpathsoffluidmaterialelementontheBernoullisurface,whereassomenewexactsolutionsareobtainedwhichareboundedinthewholeregion.Thefirstoneisacontinuedumbrellavortexsolution,whichisatyphoon-likevortex.Thesecondoneisamulti-planarsolution,whichisperiodicinz-coordinate.Withineachlayer,thereisanumbrellavortexsolutionsimilartothefirstone.Theabove...
简介:ThisstudypresentsanovelprocessofinsitusurfacemodificationofCaCChnanoparticlesusingamultipleorificedispersionmicroreactor.CO2/Ca(OH)2precipitationreactionwasemployedtoprepareCaCO3nanoparticleswithsodiumstearatesurfactant.SynthesizedCaCChproductswerecharacterizedbythermogravimetricanalysis(TGA),infra-red(IR),X-raydiffraction(XRD),transmissionelectronmicroscopy(TEM)andBrunauer-Emmet-Telleranalysis(BET).Theeffectofvariousoperationparametersonnanoparticlesandthedosageofsodiumstearateweredetermined.Theresultsshowedthatthepreparationprocesscouldbepreciselycontrolledwithefficientmasstransferprocess.Theparticleswerehighlyhydrophobicwithacontactangleof117andmonodispersewithanaveragesizeof30nm.Theadsorptionsofsodiumstearateandcalciumiononsolidparticlesduringtheinsitusurfacemodificationprocesswereinvestigated.
简介:AnovelmethodformodelingcellularmaterialsisproposedbasedonMATLABimageprocessingandsynchrotronX-raycomputedtomographyscanningtoobtainanaccuratecalculationresultofaluminumfoambasedonfiniteelementmodel.Themaximumentropyalgorithmisemployedtoobtainthebinarizationimage,andthemedianfilteringalgorithmisusedtoreducethenoiseafterbinarization.Theexternalcontourandinternalporesboundaryisextractedbythe"edge"functioninMATLAB,andthegeometricalmodelisreconstructed.Atwo-stepmeshalgorithmisadoptedtomeshthereconstructedgeometricalmodel.Accordingly,thefiniteelementmodelofaluminumfoamisestablishedbytheproposedmethodbasedonreconstructiongeometricalmodel.Thecompressionbehaviorofaluminumfoamisobtainedat25℃,100℃,200℃byABAQUS,andgoodagreementswithexperimentsareachievedbyapplyingthepresentreconstructionalgorithmandmodelingmethod.
简介:3-degree-of-freedom(3-DOF)的一个新分析模型旋转罗盘加速表系统由一个1-DOF驱动器和2-DOF感觉模式组成被介绍。模型构造微分方程由向量分析与系统的每DOF联系了的lumped。因此建立的联合微分方程是为他们在时间和频率领域的回答的解决的经分解。就这些频率反应方程而言,新奇设备设计概念被强迫感觉阶段到零导出,它导致在结构的频率之间的某个关系,从而在系统的表演上引起抑制效果的最小化。而且,现在的旋转罗盘加速表结构的可行性在他们的事件为旋转罗盘行动和线性加速的察觉用一个唯一的差别对待的计划被学习。这个计划把旋转罗盘加速表的提出的解决的短暂解决方案与同步解调和过滤的进程相结合,它导致同相并且系统输出的照部件发信号。这二个部件能在尖运动和线性加速的察觉被利用。获得的分析结果被模拟在MATLAB/Simulink环境验证,并且结果在对对方的优秀同意,这被发现。