简介:Pr2Fe14B-La2Fe14B系统被衍射(XRD),微分扫描热量测定(DSC)和扫描电子显微镜学(SEM)与精力装备了的X光检查粉末调查散X光检查光谱学(版本)。水晶结构参数被完整侧面的Rietveld精炼决定。结果揭示了那所有合金(Pr1-xLax)2Fe14B使Nd2Fe14有空格组P42/mnm的B类型结构并且形成了连续固体在x=0.0之间的解决方案并且1.0。格子参数一,c,单位房间体积V和c/a比率与La集中线性地增加了。由thermogravimetry分析决定了,居里温度(TC),阶段转变温度和融化的温度(Pr1-xLax)2Fe14B在La内容之上线性地减少了。基于DSC大小和X光检查粉末衍射考试的结果,Pr2Fe14B-La2Fe14B系统被建立。
简介:Magnetizationanddemagnetizationcurvesandhysteresisloopsapplieddifferentmagnetizing.fieldsinsinteredNd-Fe-BandNd-Dy-Fe-Bmagnetsfromthermallydemagnetizedanddcfield-demagnetizedstateswereinvestigatedattemperaturesofupto150℃.Thefirst-quadrantremagnetizationcurvesandthecurvesofcoerciveforces_MH_CversusrernagnetizingfietdsH_mfromdcfield-demagnetizedstateatroomtemperatureshowasteparoundmagnetizingfieldasabsolutevalueofthemaximumintrinsiccoercivity.Thestepsof_MH_C-H_mcurvesshiftedtolowerremagnetizingfieldsandtheshapesofmagnetizationcurveschangedfromsteptypetoprecipitoustypewhentemperaturewentupto100~150℃orafterthespecimenwasthermallydemagnetizedatatemperaturehigherthantheCurietemperature.Thesteepriseofkneecoereivitywithincreasingmagnetizingfieldisbehindthatof_MH_C.NotethatthemagnetichardeninginsinteredNd-Fe-Bmagnetsiscontrolledbypinningofdomainwalls.
简介:代号为B312的苯乙烯膦酸单仲烷基(C11-13)酯的实用性质表明,B312符合工业萃取剂所应具备的条件。
简介:Microporoustitaniumdioxidefilmswerepreparedbythesol-gelmethodsonglasssubstrates,usingtetrabutyltitanateassourcematerial.Inordertoabsorbthevisiblelightandincreasethephotocatalyticactivities,differentconcentrationsofneodymiumions(Nd/Timolarratiowas0.5%,0.7%,0.9%,and1.1%respectively)wereaddedintothesol.X-raydiffraction(XRD),X-rayphotoelectronspectros-copy(XPS),andatomforcemicroscopy(AFM)wereappliedtocharacterizethemodifiedfilms.Akindoftypicaltextileindustrypollutant(RhodamineB)wasusedtoevaluatethephotocatalyticactivitiesofthefilmsundervisiblelight.TheresultsshowedthattheactivitiesofthefilmswereimprovedbydopingNdionsintothesol.