Synthesis and Structure of the First Protonated Zincoborophosphate：（ H3O ） Zn（ H2O ） 2BP2O8·H2O-中国期刊网

摘要 Thesolidaddofthefirstprotonatedzincoborophosphate,(H3O)Zn(H2O)2BP2O8·H2O(1),wassoventothermallysyn-thesizedbythereactionofZn(NO3)2·6H2OandH3BO3withH3PO4inamixedsolvent,andstructurallycharacterizedbysingle-ystalX-raydiffractionanalysis.ItcrystallizesinthehexagonalP6122,a=0.9604(4)nm,c=1.5297(6)nm,V=1.2218(8)nm^3,Dc=2.921g/cm^3,Z=6,F(000)=1080,μ=3.495mm^-1.Thestmchwefeaturesthatthetetrahedra-te-trahedrahdlcesinterconnectedbyoctahedraandstronghydro-gembondinteractionsformathree-dimensionalframework.Theprotonatedwatermoleculesarelocatedatuniquepositions.othercharacterizationsbyIRandthermalanalysisarealsode-scribed.

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Synthesis and Structure of the First Protonated Zincoborophosphate：（ H3O ） Zn（ H2O ） 2BP2O8·H2O

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Synthesis and Structure of the First Protonated Zincoborophosphate：（ H3O ） Zn（ H2O ） 2BP2O8·H2O

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